SPECTRO ARCOS

The new SPECTRO ARCOS ICP-OES analyzer represents a new pinnacle of productivity and performance for inductively coupled plasma optical emission spectrometers

  • OVERVIEW +


    • One instrument instead of two: Only MultiView plasma instrument in the market ‒ true axial AND true radial plasma observation in a single instrument
    • ORCA Optical System: Simultaneous spectrum capture in the 130-770 nm wavelength range with up to 5x more sensitivity than Echelle based systems - delivers best in class performance in the UV/VUV range
    • LDMOS Generator: Up to 2000 W power and robust enough to handle volatile organics and high dissolved solids with ease
       

    The SPECTRO ARCOS ICP-OES excels in industrial and academic applications for the most advanced elemental analysis of metals, chemicals, petrochemicals, and other materials.

    The periscope-free MultiView mechanism lets an operator literally "turn" a radial-view instrument into an axial-view device, or vice-versa, in 90 seconds or less.

    The design of the SPECTRO ARCOS ensures exceptionally low operating costs over a long, reliable service life. And it packs a modern, ergonomic chassis with proven features such as no-purge UV-PLUS sealed gas purification technology, no-external-cooling OPI-Air Interface.

    Additional ICP-OES / ICP-AES instruments in SPECTRO’S comprehensive product line include SPECTROGREEN and SPECTRO GENESIS.

  • ON-DEMAND WEBINARS +


    You will find SPECTRO ARCOS related webinars in our resource library.
  • Q & A MULTIVIEW +


    Q & A Multiview
    Is there any sort of optical alignment necessary when switching from axial- to radial-view?
    No, the system is self-aligning.

    Is viewing height adjustable in radial-view instruments or in MultiView running in radial mode?
    The view height in radial mode is factory-optimized for best SNR.

    How can you do without an external cooling system in an axial view?
    The axial interface is surrounded by cooling fins that dissipate the heat via a stream of forced air.

    Is a dedicated axial-/radial-view ARCOS upgradable to MultiView?
    Yes, in principle it is possible. However, it would require changing the instrument’s entire single-view mechanics to a MultiView mechanism.

    With the parts disassembled and reassembled to change the orientation of the plasma, how do you ensure the precision of a measurement?
    The mechanical construction is such that optimal alignment is fully maintained. Thus the unit’s measurement precision is not affected by the disassembly/assembly of the interface and sample introduction components.

    When switching axial to radial, is the same torch required? Or is there a different torch for the axial and radial viewing modes?
    Radial and axial torches are different. A radial torch uses a straight glass body and typically a 1.8 mm injector tube. The axial torch has a slightly longer glass body, with a tulip-shaped end. Typically it uses a 2 mm injector tube.

    Is there something to be done to realign the torch after rotating the load coil? Is it possible to run the instrument with a nonaligned torch?
    The torch is self-aligning using a bayonet coupling. When the coupling is fully engaged, the torch is fully aligned. Plasma start is only possible when the coupling is fully engaged.

    How do you bracket in high-precision analysis for major components?
    Bracketing can be performed using the Smart Analyzer Vision instrument software. The concentration of bracketing element defines the standards to be used. The bracketing measurements are performed per the defined number of cycles. After that, the bracketing correction is automatically calculated and applied to the unknown sample.

    For the MultiView instrument, is torch alignment within the software using an Mn standard required each time you change the orientation of the torch?
    No. An optimization, which can be performed automatically, is only required if sample introduction components are changed — e.g. if a different nebulizer or spray chamber is used.

    Does the sample have to be solubilized into a solution for ICP analysis?

    Yes — in general ICP is a solution technique.

    What is the effect of the type of spray chamber used on sensitivity … and the results presented?
    Sensitivity is mainly affected by the nebulizer and only to a lesser extent by the spray chamber. The type of spray chamber used influences washout and precision, however. For example, plastic spray chambers do not drain very well, which has a negative effect on precision; small cyclonic spray chambers have a faster washout; large-volume spray chambers have the best long-term stability.

    Is it possible to use MultiView with all available sample introduction systems?
    Yes, absolutely. There are no limitations in this regard.

    Is your torch one-piece or demountable?

    One-piece and demountable torches are available.

    Is a dual-view axial analysis equivalent to axial-only instrumentation? If it is, wouldn’t it be a better choice when choosing between axial- and dual-view?
    Sensitivity-wise, there is no difference between axial dual-view and dedicated dual-view. A dedicated axial system is typically less expensive, however. So when a radial mode is not needed, money can be saved. Should it be necessary, the SPECTRO dual-view (Twin Interface) is field-upgradable at any later point in time.

    In a dual-view system, what is the approximate loss of performance in the radial view?
    In the wavelength range between 165 and 285 nm, sensitivity is about a factor of 2 lower compared to a dedicated radial view. Above 285 nm, there is no difference in sensitivity.

    Is it necessary to optimize the torch’s positions or does it use fixed positions?
    The system uses fixed, factory-optimized positions.

    Is there any disadvantage to axial-view when analyzing high HF solutions?

    No, high HF solutions do not affect the axial interface.

    What are the cost comparisons of dual/radial/axial/MV?
    Radial and axial are about the same price. Dual-view adds about 5% to the overall cost. MultiView also adds about 5% to the cost of the ARCOS system.

    When calibrating using a multi-element mix, is there a choice of selecting radial view for alkali metals and axial for the rest of the elements?
    When using an ICP with dual-view plasma observation, the typical method of operation is to analyze wavelengths below 285 nm using the axial mode, because metals have their most prominent lines in this wavelength range. This provides the highest sensitivity. Also, those elements/lines are not affected by the EIE effect. Wavelengths above 285 nm are typically analyzed using the radial mode. For the group 1 and 2 elements, there is little need to analyze trace levels, and even in radial mode the sensitivity is still high. While those elements are strongly affected by the EIE effect, the radial mode is beneficial since it greatly reduces the effect. Certainly, if desired, the entire spectrum can be analyzed radially as well as axially.

    What is the detection limit with MultiView?
    It is the same as with a dedicated axial or a dedicated radial.

    Can the same sample be run in both views on the MultiView? If so, do you need to run calibration standards for each view or is a common one enough for both views?
    That is certainly possible. Calibration standards can be the same, but since the plasma view is completely different, radial- and axial-view require different calibrations.

    Will you please explain a little more about the effect of the nebulizer and its relevance to the particular view mode?
    The nebulization of the sample is independent of the viewing mode. Using a pneumatic nebulizer, the efficiency is between 2% and 5%, so the same amount of sample enters the plasma. What is different is that in radial mode only a cross section of the plasma is viewed, while in axial mode the entire excitation zone is viewed and more light is transferred into the optic. Therefore, sensitivity is higher compared to the radial mode.

    Which mode would you recommend for S measurements at 182 nm?
    Both modes are suitable. The observation direction really depends on the application. E.g., for analyzing sulfur in organic solutions, radial is preferred; however, traces of sulfur in an aqueous matrix are better analyzed using the axial mode. Axial provides better LODs.

    Does dual-view mean that there are two light beams?
    Yes, that is true. For highest performance, dual-view systems use an automatic sequential measurement to analyze the sample using an axial and a radial light path. Simultaneous dual-view also exists; however, this capability comes at the cost of a compromised performance.

    For chlorine (Cl) analysis, which view mode is best? What are the detection limits?

    For the analysis of Cl in a clean aqueous matrix, an LOD of 30 ppb can be achieved with axial and 100 ppb with radial plasma observation. Which is more suitable depends on the application and the required sensitivity. For an application with higher amounts of totally dissolved solids and for organic solutions, radial plasma observation is preferred.
  • VIDEO +

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  • BROCHURES +

  • WHITEPAPERS +

  • APPLICATIONS +

    Application Reports
  • MORE INFO +

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  • USER MANUAL +